Xinjiang Agricultural Sciences ›› 2022, Vol. 59 ›› Issue (3): 674-682.DOI: 10.6048/j.issn.1001-4330.2022.03.017
• Plant Protection·Agricultural Product Analysis and Detection • Previous Articles Next Articles
ZHANG Rui1,2(), GOU Chunlin3, WANG Zhi2, QIAO Kunyun2, YUAN Yuwei4, NIE Jing4, JU Yanjun2, ZHAO Duoyong2()
Received:
2021-08-15
Online:
2022-03-20
Published:
2022-03-28
Correspondence author:
ZHAO Duoyong
Supported by:
张瑞1,2(), 苟春林3, 王智2, 乔坤云2, 袁玉伟4, 聂晶4, 琚艳君2, 赵多勇2()
通讯作者:
赵多勇
作者简介:
张瑞(1997-),女,吉林松原人,硕士研究生,研究方向为食品加工与安全,(E-mail) 1761262569@qq.com
基金资助:
CLC Number:
ZHANG Rui, GOU Chunlin, WANG Zhi, QIAO Kunyun, YUAN Yuwei, NIE Jing, JU Yanjun, ZHAO Duoyong. Geographical Origin Discrimination of Jinghe Wolfberry and Zhongning Wolfberry Based on Multi Mineral Elements Analysis[J]. Xinjiang Agricultural Sciences, 2022, 59(3): 674-682.
张瑞, 苟春林, 王智, 乔坤云, 袁玉伟, 聂晶, 琚艳君, 赵多勇. 基于多种矿物元素的精河枸杞与中宁枸杞产地鉴别[J]. 新疆农业科学, 2022, 59(3): 674-682.
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URL: http://www.xjnykx.com/EN/10.6048/j.issn.1001-4330.2022.03.017
仪器名称 Name of instrument | 型号 Model | 生产厂家 Manufacturers |
---|---|---|
电感耦合等离子体质谱 ICP-MS | 7700X | 美国Agilent科技公司 |
微波消解仪 Microwave Digester | Mars240/50 | 美国CEM公司 |
超纯水仪 Ultra-pure water meter | Cascada III.I20 | 美国Pall公司 |
酸纯化仪 Acid Purification Instrument | DST-1000 | 美国Savillex公司 |
破壁机 Wall breaker | HR3868 | 荷兰Philips电子公司 |
电子天平 Electronic balance | XSE204 | 瑞士Mettler公司 |
Table 1 Main instruments and manufacturers
仪器名称 Name of instrument | 型号 Model | 生产厂家 Manufacturers |
---|---|---|
电感耦合等离子体质谱 ICP-MS | 7700X | 美国Agilent科技公司 |
微波消解仪 Microwave Digester | Mars240/50 | 美国CEM公司 |
超纯水仪 Ultra-pure water meter | Cascada III.I20 | 美国Pall公司 |
酸纯化仪 Acid Purification Instrument | DST-1000 | 美国Savillex公司 |
破壁机 Wall breaker | HR3868 | 荷兰Philips电子公司 |
电子天平 Electronic balance | XSE204 | 瑞士Mettler公司 |
步骤 Steps | 温度 Temperature (℃) | 爬升时间 Climbing time (min) | 保持时间 Maintain time (min) | 功率 Power (W) | |
---|---|---|---|---|---|
升温 Heat up | 1 | 120 | 8 | 2 | 1 600 |
2 | 160 | 5 | 5 | 1 600 | |
降温 Cooling | 3 | 180 | 5 | 15 | 1 600 |
4 | - | 20 | - | - |
Table 2 Microwave digestion parameters
步骤 Steps | 温度 Temperature (℃) | 爬升时间 Climbing time (min) | 保持时间 Maintain time (min) | 功率 Power (W) | |
---|---|---|---|---|---|
升温 Heat up | 1 | 120 | 8 | 2 | 1 600 |
2 | 160 | 5 | 5 | 1 600 | |
降温 Cooling | 3 | 180 | 5 | 15 | 1 600 |
4 | - | 20 | - | - |
名称 Name | 参数 Parameter | 名称 Name | 参数 Parameter |
---|---|---|---|
RF功率 RF power | 1 350 W | 雾化室温度 Temperature of atomizing chamber | 2℃ |
采样深度 Sampling depth | 7.5 mm | 冷却气流速 Cooling gas velocity | 15 L/min |
辅助气流速 Auxiliary gas velocity | 1.0 L/min | 载气速度 Gas carrier velocity | 1.14 L/min |
氧化物指标 Oxide indicators | CeO+/Ce+<1.5% | 双电荷指标 Double charge indicator | Ce2+/Ce+<3% |
Table 3 Working parameters of ICP-MS
名称 Name | 参数 Parameter | 名称 Name | 参数 Parameter |
---|---|---|---|
RF功率 RF power | 1 350 W | 雾化室温度 Temperature of atomizing chamber | 2℃ |
采样深度 Sampling depth | 7.5 mm | 冷却气流速 Cooling gas velocity | 15 L/min |
辅助气流速 Auxiliary gas velocity | 1.0 L/min | 载气速度 Gas carrier velocity | 1.14 L/min |
氧化物指标 Oxide indicators | CeO+/Ce+<1.5% | 双电荷指标 Double charge indicator | Ce2+/Ce+<3% |
序号 Num | 元素 Elements | 新疆精河县 Jinghe County, Xinjiang (n=50) | 宁夏中宁县 Zhongning County, Ningxia (n=52) |
---|---|---|---|
$\bar{X}±S$ | X$\bar{X}±S$ | ||
1 | B | 2.04±0.45 | 1.99±0.30 |
2 | Na** | 601.31±205.24 | 842.18±450.94 |
3 | Mg** | 216.32±24.89 | 189.50±37.30 |
4 | Al** | 3 338.44±1 074.98 | 2 713.58±817.92 |
5 | P** | 561.45±73.54 | 504.86±91.12 |
6 | K** | 4 188.94±358.23 | 3 358.26±438.15 |
7 | Ca** | 180.83±44.81 | 225.77±56.05 |
8 | V** | 8.70±3.20 | 6.94±2.41 |
9 | Cr | 67.51±84.59 | 51.94±25.51 |
10 | Mn | 1 870.07±240.73 | 1 750.91±431.99 |
11 | Fe | 13.01±4.04 | 12.36±4.89 |
12 | Co | 11.17±4.16 | 10.06±3.23 |
13 | Ni** | 178.87±63.69 | 213.76±71.26 |
14 | Cu** | 2 126.10±616.73 | 1 385.47±662.86 |
15 | Zn** | 4 261.70±2 402.81 | 2 985.83±883.39 |
16 | As** | 5.72±1.91 | 4.75±1.49 |
17 | Se* | 18.48±20.08 | 11.66±4.86 |
18 | Rb** | 222.22±112.29 | 493.28±353.98 |
序号 Num | 元素 Elements | 新疆精河县 Jinghe County, Xinjiang (n=50) | 宁夏中宁县 Zhongning County, Ningxia (n=52) |
$\bar{X}±S$ | $\bar{X}±S$ | ||
19 | Sr* | 1 221.06±474.20 | 1 719.74±1 019.57 |
20 | Mo** | 77.01±18.71 | 35.23±11.06 |
21 | Pd | 0.82±0.31 | 0.83±0.32 |
22 | Ag* | 16.66±8.15 | 14.90±7.59 |
23 | Cd** | 14.77±6.51 | 11.00±9.06 |
24 | Sb | 1.07±0.70 | 1.06±0.72 |
25 | Cs | 1.2±0.47 | 1.58±1.15 |
26 | Ba | 199.58±74.93 | 216.85±80.20 |
27 | La | 4.96±1.91 | 4.75±1.87 |
28 | Ce | 5.75±3.21 | 5.09±2.68 |
29 | Pr | 1±0.45 | 0.87±0.34 |
30 | Nd | 3.88±1.77 | 3.45±1.29 |
31 | Sm | 0.73±0.37 | 0.66±0.28 |
32 | Eu | 0.13±0.08 | 0.11±0.06 |
33 | Gd* | 0.65±0.31 | 0.52±0.22 |
34 | Dy | 0.48±0.20 | 0.44±0.19 |
35 | Ho | 0.07±0.04 | 0.06±0.04 |
36 | Er** | 0.19±0.11 | 0.13±0.09 |
37 | Tm | 0.03±0.02 | 0.03±0.02 |
38 | Yb | 0.25±0.10 | 0.22±0.08 |
39 | Hf** | 1.26±0.44 | 1.96±0.70 |
40 | Ir** | 0.11±0.07 | 0.20±0.10 |
41 | Pt | 0.08±0.05 | 0.08±0.05 |
42 | Au** | 1.36±0.25 | 1.75±0.35 |
43 | Tl** | 0.26±0.20 | 0.40±0.18 |
44 | Pb** | 36.80±18.38 | 29.16±15.01 |
45 | Th** | 3.01±7.88 | 5.91±12.13 |
46 | U** | 1.76±0.42 | 0.71±0.22 |
Table 4 Contents of 46 elements of wolfberry
序号 Num | 元素 Elements | 新疆精河县 Jinghe County, Xinjiang (n=50) | 宁夏中宁县 Zhongning County, Ningxia (n=52) |
---|---|---|---|
$\bar{X}±S$ | X$\bar{X}±S$ | ||
1 | B | 2.04±0.45 | 1.99±0.30 |
2 | Na** | 601.31±205.24 | 842.18±450.94 |
3 | Mg** | 216.32±24.89 | 189.50±37.30 |
4 | Al** | 3 338.44±1 074.98 | 2 713.58±817.92 |
5 | P** | 561.45±73.54 | 504.86±91.12 |
6 | K** | 4 188.94±358.23 | 3 358.26±438.15 |
7 | Ca** | 180.83±44.81 | 225.77±56.05 |
8 | V** | 8.70±3.20 | 6.94±2.41 |
9 | Cr | 67.51±84.59 | 51.94±25.51 |
10 | Mn | 1 870.07±240.73 | 1 750.91±431.99 |
11 | Fe | 13.01±4.04 | 12.36±4.89 |
12 | Co | 11.17±4.16 | 10.06±3.23 |
13 | Ni** | 178.87±63.69 | 213.76±71.26 |
14 | Cu** | 2 126.10±616.73 | 1 385.47±662.86 |
15 | Zn** | 4 261.70±2 402.81 | 2 985.83±883.39 |
16 | As** | 5.72±1.91 | 4.75±1.49 |
17 | Se* | 18.48±20.08 | 11.66±4.86 |
18 | Rb** | 222.22±112.29 | 493.28±353.98 |
序号 Num | 元素 Elements | 新疆精河县 Jinghe County, Xinjiang (n=50) | 宁夏中宁县 Zhongning County, Ningxia (n=52) |
$\bar{X}±S$ | $\bar{X}±S$ | ||
19 | Sr* | 1 221.06±474.20 | 1 719.74±1 019.57 |
20 | Mo** | 77.01±18.71 | 35.23±11.06 |
21 | Pd | 0.82±0.31 | 0.83±0.32 |
22 | Ag* | 16.66±8.15 | 14.90±7.59 |
23 | Cd** | 14.77±6.51 | 11.00±9.06 |
24 | Sb | 1.07±0.70 | 1.06±0.72 |
25 | Cs | 1.2±0.47 | 1.58±1.15 |
26 | Ba | 199.58±74.93 | 216.85±80.20 |
27 | La | 4.96±1.91 | 4.75±1.87 |
28 | Ce | 5.75±3.21 | 5.09±2.68 |
29 | Pr | 1±0.45 | 0.87±0.34 |
30 | Nd | 3.88±1.77 | 3.45±1.29 |
31 | Sm | 0.73±0.37 | 0.66±0.28 |
32 | Eu | 0.13±0.08 | 0.11±0.06 |
33 | Gd* | 0.65±0.31 | 0.52±0.22 |
34 | Dy | 0.48±0.20 | 0.44±0.19 |
35 | Ho | 0.07±0.04 | 0.06±0.04 |
36 | Er** | 0.19±0.11 | 0.13±0.09 |
37 | Tm | 0.03±0.02 | 0.03±0.02 |
38 | Yb | 0.25±0.10 | 0.22±0.08 |
39 | Hf** | 1.26±0.44 | 1.96±0.70 |
40 | Ir** | 0.11±0.07 | 0.20±0.10 |
41 | Pt | 0.08±0.05 | 0.08±0.05 |
42 | Au** | 1.36±0.25 | 1.75±0.35 |
43 | Tl** | 0.26±0.20 | 0.40±0.18 |
44 | Pb** | 36.80±18.38 | 29.16±15.01 |
45 | Th** | 3.01±7.88 | 5.91±12.13 |
46 | U** | 1.76±0.42 | 0.71±0.22 |
地点 Location | 样本量 Sample size | 识别率 Recognition(%) | 新疆精河县 Jinghe County, Xinjiang | 宁夏中宁县 Zhongning County, Ningxia |
---|---|---|---|---|
新疆精河县 Jinghe County, Xinjiang | 50 | 100% | 50 | 0 |
宁夏中宁县 Zhongning County, Ningxia | 52 | 98.08% | 1 | 51 |
Table 5 Identification of evaluation form of wolfberry. from two areas
地点 Location | 样本量 Sample size | 识别率 Recognition(%) | 新疆精河县 Jinghe County, Xinjiang | 宁夏中宁县 Zhongning County, Ningxia |
---|---|---|---|---|
新疆精河县 Jinghe County, Xinjiang | 50 | 100% | 50 | 0 |
宁夏中宁县 Zhongning County, Ningxia | 52 | 98.08% | 1 | 51 |
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