Volatile aroma components analysis of seabuckthorn vacuum freeze-dried fruit powder from different varieties based on gas chromatography-mass spectrometric

doi:10.6048/j.issn.1001-4330.2023.08.017

Xinjiang Agricultural Sciences ›› 2023, Vol. 60 ›› Issue (8): 1958-1965.DOI: 10.6048/j.issn.1001-4330.2023.08.017

• Horticultural Special Local Products · Agricultural Product Processing Engineering • Previous Articles Next Articles

Volatile aroma components analysis of seabuckthorn vacuum freeze-dried fruit powder from different varieties based on gas chromatography-mass spectrometric

LIAN Yali¹(), MENG Xintao²^,³, YANG Yongxing¹, YANG Haiyan¹, ZHANG Ting²^,³, CHE Fengbin²^,³, MA Yan²^,³()

1. College of Food and Pharmaceutical Sciences, Xinjiang Agricultural University, Urumqi 830052,China
2. Research Institute of Agro-products Storage and Processing / Xinjiang Main Agricultural and Sideline Products Intensive Processing Engineering Technology Research Center, Xinjiang Academy of Agricultural Sciences, Urumqi 830052, China
3. Seabuckthorn Engineering Technology Research Center in Xinjiang, Habahe Xinjiang 830000, China

Received:2022-11-22 Online:2023-08-20 Published:2023-08-14
Correspondence author: MA Yan(1984-), female, Jinan, Shandong, Researcher, research field: Agricultural products processing,(E-mail)282568949@qq.com
Supported by:
Basic Scientific R & D Program of Public Welfare Research Institutions of Xinjiang Uygur Autonomous Region of China(Ky2021143);Special Demonstration Project for Transformation of Scientific and Technological Achievements of Xinjiang Uygur Autonomous Region(2021NC037);Special Task Project for Key R & D in Xinjiang Uygur Autonomous Region“Research and Development and Application of High Value Processing and Utilization Technology from Seabuckthorn By-products(2022B02005-3)

基于GC-IMS技术分析不同品种沙棘真空冷冻干燥果粉挥发性成分

连雅丽¹(), 孟新涛²^,³, 杨永兴¹, 杨海燕¹, 张婷²^,³, 车凤斌²^,³, 马燕²^,³()

1.新疆农业大学食品科学与药学学院,乌鲁木齐 830052
2.新疆农业科学院农产品贮藏加工研究所/新疆主要农副产品精深加工工程技术研究中心,乌鲁木齐 830091
3.新疆沙棘工程技术研究中心,新疆哈巴河 830000

通讯作者: 马燕(1984-),女,山东济南人,研究员,博士,研究方向为农产品加工,(E-mail)282568949@qq.com
作者简介:连雅丽(1996-),女,新疆奎屯人,硕士研究生,研究方向为农产品加工,(E-mail)1004817296@qq.com
基金资助:
新疆维吾尔自治区公益性科研院所基本科研业务专项(Ky2021143);新疆维吾尔自治区科技成果转化示范专项(2021NC037);自治区重点研发任务专项课题(沙棘副产品高值化加工利用技术研发及应用)(2022B02005-3)

Abstract

Abstract:

【Objective】 To research different species of seabuckthorn producing volatile aroma composition in the hope of providing the scientific basis for comprehensive utilization of seabuckthorn plant resources.【Methods】 Characteristic aroma of seabuckthorn fruit powder from different species was analyzed by GC-IMS(Gas chromatography-ion mobility spectroscopy, GC-IMS).【Results】 A total of 56 volatile substances were detected in seabuckthorn fruit powder from 6 varieties, which 38 kinds of qualitative material were characterized, mainly esters, alcohols, aldehydes, etc.The contribution rate of PC₁ was 44%, PC₂ was 26% and the cumulative contribution rate was 70%, which could better reflect the differences among seabuckthorn fruit powder from different varieties.【Conclusion】 There were differences in volatile substances of seabuckthorn fruit powder among 6 varieties, The volatile substances of yellow fruit seabuckthorn fruit powder and yellow bag fruit seabuckthorn fruit powder, champion yellow seabuckthorn fruit powder and red big fruit seabuckthorn fruit powder are similar by fingerprint and PCA analysis.

Key words: GC-IMS; seabuckthorn fruit powder; volatile components

摘要：

【目的】研究不同品种沙棘果粉挥发性香气成分,为沙棘植物资源综合利用提供科学依据。【方法】采用气相离子迁移谱(Gas chromatography-ion mobility spectroscopy, GC-IMS)技术,分析不同品种沙棘果粉的特征香气。【结果】6个品种沙棘果粉共检出56个挥发性香气物质,其中定性了38个物质,主要为酯类、醇类、醛类等;主成分1(PC₁)和主成分2(PC₂)贡献率分别为44%和26%,累计贡献率为70%,能较好地反映不同品种沙棘果粉的差异。【结论】6个品种沙棘果粉挥发性物质存在差异,黄色果沙棘果粉和黄色袋果沙棘果粉,状元黄沙棘果粉和红色大果沙棘果粉的挥发性香气物质较为相似。

关键词: 气相离子迁移色谱(GC-IMS), 沙棘果粉, 挥发性成分

CLC Number:

S609

LIAN Yali, MENG Xintao, YANG Yongxing, YANG Haiyan, ZHANG Ting, CHE Fengbin, MA Yan. Volatile aroma components analysis of seabuckthorn vacuum freeze-dried fruit powder from different varieties based on gas chromatography-mass spectrometric[J]. Xinjiang Agricultural Sciences, 2023, 60(8): 1958-1965.

连雅丽, 孟新涛, 杨永兴, 杨海燕, 张婷, 车凤斌, 马燕. 基于GC-IMS技术分析不同品种沙棘真空冷冻干燥果粉挥发性成分[J]. 新疆农业科学, 2023, 60(8): 1958-1965.

Figures/Tables 6

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编号 Number	化合物英文名称 Compound English name	化合物中文名称 Compound Chinese name		溴代二氯甲烷CAS号		分子式 Molecular formula		保留指数 Retention index		保留时间 Retention time(s)		漂移时间 Drift time (ms)
1	Ethyl hexanoate	正己酸乙酯(二聚体)		C123660		C₈H₁₆O₂		1 007		657.367		1.344 4
2	heptanal	庚醛		C111717		C₇H₁₄O		891.7		426.069		1.349 2
3	acetoin	3-羟基-2-丁酮(二聚体)		C513860		C₄H₈O₂		721		225.263		1.508 1
4	Styrene	苯乙烯		C100425		C₈H₈		891		424.883		1.442 3
5	3-Hexen-1-ol,(E)-	反式-3-己烯-1-醇		C928972		C₆H₁₂O		840.3		351.449		1.261
6	1-Hexanol	正己醇(单体)		C111273		C₆H₁₄O		862.5		381.876		1.329 9
7	propyl bytanoate	丁酸丙酯		C105668		C₇H₁₄O₂		891.7		426.069		1.697 5
8	Alpha-Terpinene	松油烯		C99865		C₁₀H₁₆		1 019.6		689.393		1.216
9	Butanoic acid 3-methyl- 3-methylbutyl ester	异戊酸异戊酯(单体)		C659701		C₁₀H₂₀O₂		1 100.3		934.925		1.464 8
10	2-Heptenal, (E)-	E-2-庚烯醛		C18829555		C₇H₁₂O		954.9		540.279		1.252 9
11	Thiazole	噻唑		C288471		C₃H₃NS		755.1		255.691		1.251 8
12	Ethyl butanoate	丁酸乙酯(单体)		C105544		C₆H₁₂O₂		789.8		290.935		1.208 4
13	2-methylpyrazine	2-甲基吡嗪		C109080		C₅H₆N₂		818.3		323.706		1.080 5
14	Hexyl acetate	乙酸己酯		C142927		C₈H₁₆O₂		1 004.8		652.146		1.425 3
15	2-octanol	仲辛醇		C123966		C₈H₁₈O		1 009.9		664.675		1.843 7
16	Butanoic acid 3-methyl- 3-methylbutyl ester	异戊酸异戊酯(二聚体)		C659701		C₁₀H₂₀O₂		1 099.6		932.553		2.026 6
17	octanal	正辛醛		C124130		C₈H₁₆O		1 012.4		670.939		1.385 1
18	ethyl acetate	乙酸乙酯		C141786		C₄H₈O₂		599.2		143.825		1.323
19	4-Methyl-1-pentanol	4-甲基-1-戊醇		C626891		C₆H₁₄O		845.1		357.713		1.308 1
20	(E)-2-hexen-1-ol	反式-2-己烯醇		C928950		C₆H₁₂O		866.8		388.141		1.161
21	1-Hexanol	正己醇(二聚体)		C111273		C₆H₁₄O		861.9		380.982		1.643 7
22	2-butanone	2-丁酮		C78933		C₄H₈O		587		137.56		1.231 1
23	butanal		正丁醛		C123728		C₄H₈O		590.5		139.35		1.283 9
24	2,3-pentanedione		2,3-戊二酮		C600146		C₅H₈O₂		702.1		210.05		1.205 8
25	acetoin		3-羟基-2-丁酮(单体)		C513860		C₄H₈O₂		722.1		226.158		1.248 3
26	3-Methyl-2-butanol		3-甲基-2-丁醇		C598754		C₅H₁₂O		695.1		204.68		1.228 8
27	ethyl 2-methylbutanoate		2-甲基丁酸乙酯		C7452791		C₇H₁₄O₂		838.4		348.97		1.654 2
28	6-methyl-5-hepten-2-one		6-甲基-5-庚烯-2-酮		C110930		C₈H₁₄O		993.7		625.341		1.172 7
29	3-Methylpentanol		3-甲基-1-戊醇		C589355		C₆H₁₄O		838.3		348.764		1.602 3
30	Propanoic acid		丙酸		C79094		C₃H₆O₂		690.3		201.1		1.265 6
31	Pentanal		正戊醛		C110623		C₅H₁₀O		719.9		224.369		1.398 9
32	Ethyl butanoate		丁酸乙酯(二聚体)		C105544		C₆H₁₂O₂		782.5		283.155		1.558 5
33	2-methyl-3-(methylthio)furan		2-甲基-3-甲硫基呋喃		C63012975		C₆H₈OS		949.4		529.264		1.145 4
34	2-methylpropanoic acid		异丁酸		C79312		C₄H₈O₂		779.7		280.238		1.371 6
35	1,4-dioxane		1,4-二氧六环		C123911		C₄H₈O₂		698.6		207.365		1.324 2
36	ethyl 2-methylbutanoate		2-甲基丁酸乙酯		C7452791		C₇H₁₄O₂		847.7		361.293		1.226 5
37	Ethyl hexanoate		正己酸乙酯(单体)		C123660		C₈H₁₆O₂		1 007		657.367		1.344 4
38	beta-Ocimene		罗勒烯		C13877913		C₁₀H₁₆		1 044		755.817		1.206 4

编号 Number	化合物英文名称 Compound English name	化合物中文名称 Compound Chinese name		溴代二氯甲烷CAS号		分子式 Molecular formula		保留指数 Retention index		保留时间 Retention time(s)		漂移时间 Drift time (ms)
1	Ethyl hexanoate	正己酸乙酯(二聚体)		C123660		C₈H₁₆O₂		1 007		657.367		1.344 4
2	heptanal	庚醛		C111717		C₇H₁₄O		891.7		426.069		1.349 2
3	acetoin	3-羟基-2-丁酮(二聚体)		C513860		C₄H₈O₂		721		225.263		1.508 1
4	Styrene	苯乙烯		C100425		C₈H₈		891		424.883		1.442 3
5	3-Hexen-1-ol,(E)-	反式-3-己烯-1-醇		C928972		C₆H₁₂O		840.3		351.449		1.261
6	1-Hexanol	正己醇(单体)		C111273		C₆H₁₄O		862.5		381.876		1.329 9
7	propyl bytanoate	丁酸丙酯		C105668		C₇H₁₄O₂		891.7		426.069		1.697 5
8	Alpha-Terpinene	松油烯		C99865		C₁₀H₁₆		1 019.6		689.393		1.216
9	Butanoic acid 3-methyl- 3-methylbutyl ester	异戊酸异戊酯(单体)		C659701		C₁₀H₂₀O₂		1 100.3		934.925		1.464 8
10	2-Heptenal, (E)-	E-2-庚烯醛		C18829555		C₇H₁₂O		954.9		540.279		1.252 9
11	Thiazole	噻唑		C288471		C₃H₃NS		755.1		255.691		1.251 8
12	Ethyl butanoate	丁酸乙酯(单体)		C105544		C₆H₁₂O₂		789.8		290.935		1.208 4
13	2-methylpyrazine	2-甲基吡嗪		C109080		C₅H₆N₂		818.3		323.706		1.080 5
14	Hexyl acetate	乙酸己酯		C142927		C₈H₁₆O₂		1 004.8		652.146		1.425 3
15	2-octanol	仲辛醇		C123966		C₈H₁₈O		1 009.9		664.675		1.843 7
16	Butanoic acid 3-methyl- 3-methylbutyl ester	异戊酸异戊酯(二聚体)		C659701		C₁₀H₂₀O₂		1 099.6		932.553		2.026 6
17	octanal	正辛醛		C124130		C₈H₁₆O		1 012.4		670.939		1.385 1
18	ethyl acetate	乙酸乙酯		C141786		C₄H₈O₂		599.2		143.825		1.323
19	4-Methyl-1-pentanol	4-甲基-1-戊醇		C626891		C₆H₁₄O		845.1		357.713		1.308 1
20	(E)-2-hexen-1-ol	反式-2-己烯醇		C928950		C₆H₁₂O		866.8		388.141		1.161
21	1-Hexanol	正己醇(二聚体)		C111273		C₆H₁₄O		861.9		380.982		1.643 7
22	2-butanone	2-丁酮		C78933		C₄H₈O		587		137.56		1.231 1
23	butanal		正丁醛		C123728		C₄H₈O		590.5		139.35		1.283 9
24	2,3-pentanedione		2,3-戊二酮		C600146		C₅H₈O₂		702.1		210.05		1.205 8
25	acetoin		3-羟基-2-丁酮(单体)		C513860		C₄H₈O₂		722.1		226.158		1.248 3
26	3-Methyl-2-butanol		3-甲基-2-丁醇		C598754		C₅H₁₂O		695.1		204.68		1.228 8
27	ethyl 2-methylbutanoate		2-甲基丁酸乙酯		C7452791		C₇H₁₄O₂		838.4		348.97		1.654 2
28	6-methyl-5-hepten-2-one		6-甲基-5-庚烯-2-酮		C110930		C₈H₁₄O		993.7		625.341		1.172 7
29	3-Methylpentanol		3-甲基-1-戊醇		C589355		C₆H₁₄O		838.3		348.764		1.602 3
30	Propanoic acid		丙酸		C79094		C₃H₆O₂		690.3		201.1		1.265 6
31	Pentanal		正戊醛		C110623		C₅H₁₀O		719.9		224.369		1.398 9
32	Ethyl butanoate		丁酸乙酯(二聚体)		C105544		C₆H₁₂O₂		782.5		283.155		1.558 5
33	2-methyl-3-(methylthio)furan		2-甲基-3-甲硫基呋喃		C63012975		C₆H₈OS		949.4		529.264		1.145 4
34	2-methylpropanoic acid		异丁酸		C79312		C₄H₈O₂		779.7		280.238		1.371 6
35	1,4-dioxane		1,4-二氧六环		C123911		C₄H₈O₂		698.6		207.365		1.324 2
36	ethyl 2-methylbutanoate		2-甲基丁酸乙酯		C7452791		C₇H₁₄O₂		847.7		361.293		1.226 5
37	Ethyl hexanoate		正己酸乙酯(单体)		C123660		C₈H₁₆O₂		1 007		657.367		1.344 4
38	beta-Ocimene		罗勒烯		C13877913		C₁₀H₁₆		1 044		755.817		1.206 4

Volatile aroma components analysis of seabuckthorn vacuum freeze-dried fruit powder from different varieties based on gas chromatography-mass spectrometric

基于GC-IMS技术分析不同品种沙棘真空冷冻干燥果粉挥发性成分

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