大白菜中氟氯氰菊酯残留的快速测定及方法评估

doi:10.6048/j.issn.1001-4330.2021.01.020

新疆农业科学 ›› 2021, Vol. 58 ›› Issue (1): 168-175.DOI: 10.6048/j.issn.1001-4330.2021.01.020

• 植物保护·土壤肥料·贮藏保鲜加工·农业水土工程·微生物·农产品分析检测 • 上一篇下一篇

大白菜中氟氯氰菊酯残留的快速测定及方法评估

谭慧林¹, 金永生², 余琪¹, 牛贵洋¹, 包东东¹, 陈海元¹, 张志东³

1.阿克苏地区食品安全检测中心,新疆阿克苏 843000;
2.阿克苏地区检验检测中心,新疆阿克苏 843000;
3.新疆农业科学院微生物应用研究所/新疆特殊环境微生物实验室,乌鲁木齐 830091

收稿日期:2019-03-09 出版日期:2021-01-20 发布日期:2021-01-20
通信作者: 张志东(1977-),男,新疆乌鲁木齐人,研究员,研究方向为特殊环境微生物学和食品科学,(E-mail) zhangzheedong@qq.com
作者简介:谭慧林(1977-),女,新疆乌鲁木齐人,副高级工程师,研究方向为食品安全检验,(E-mail)45118707 @qq.com
基金资助:
国家重点研发计划(2018YFC1603400); 天山雪松计划(2017XS26)

Determination of Cynuthrin Residues in Chinese Cabbages and Evaluation of the Rapid Detection Method

TAN Huilin¹, JIN Yongsheng², YU Qi¹, NIU Guiyang¹, BAO Dongdong¹, CHEN Haiyuan¹, ZHANG Zhidong³

1. Food Safety Testing Center of Aksu Prefecture, Aksu Xinjiang 843000, China;
2. Inspection and Testing Center of Aksu Prefecture, Aksu Xinjiang 843000, China;
3. Xinjiang Laboratory of Special Environmental Microbiology/Research Institute of Applied Microbiology, Urumqi 830091, China

Received:2019-03-09 Online:2021-01-20 Published:2021-01-20
Correspondence author: ZHANG Zhidong (1977- ),male,Urumqi Xinjiang, professor, research field: Microbiology in the extraordinary environment & Food Sciences,(E-mail) zhangzheedong@qq.com
Supported by:
The National Key R & D Program Project(2018YFC1603400);Tianshang Cedar Program Project (2017XS26)

摘要/Abstract

摘要： 【目的】 检测阿克苏市市场中大白菜氟氯氰菊酯农药残留, 进行菊酯快检试剂盒在大白菜氟氯氰菊酯农药残留中适用性评估。【方法】 采用行业标准NY/T 761-2008参比方法和菊酯快检试剂盒对阿克苏市售大白菜中氟氯氰菊酯进行测定,并对菊酯快检试剂盒根据《食品快速检测方法评价技术规范》在大白菜中适用性进行评估。【结果】 所得大白菜样品经气相色谱测定,均未检出氟氯氰菊酯。根据不同加标水平检测结果分析,实验所用快检试剂盒的灵敏度75%,其对菊酯类农残具有特异性100%,其假阴性率25%,假阳性率0,试剂盒检出限为0.4 mg/kg。【结论】 阿克苏市售大白菜氟氯氰菊酯残留均低于《食品安全国家标准食品中农药最大残留限量》中限量要求,所用试剂盒适用于大白菜中氟氯氰菊酯残留的快速筛查。

关键词: 大白菜; 氟氯氰菊酯残留; 快检试剂盒; 评估

Abstract: 【Objective】 To detect cynuthrin residues in Chinese cabbages from markets of Aksu region, and evaluate the fast kit for cynuthrin.【Methods】 The reference method, industry standard NY / T 761-2008 and the rapid kit for pyrethroid were used to determine cynuthrin residues in Chinese cabbages. The rapid kit was evaluated according to "technical specification for evaluation of rapid detection methods of food".【Results】 None of cynuthrin residues was detected in all samples by the GC method. According to test results in different spiked levels for cynuthrin by the fast test kit, the sensitivity of the kit was 75%, and specificity for pyrethroid pesticide residues was 100%. Compared with the instructions, the false negative rate was 25%, the rate of false positive was 0, and the detection limit concentration was 0.4 mg/kg. 【Conclusion】 Cynuthrin residues in Chinese cabbage sold in Aksu region was lower than the maximum residue limit allowed. The fast kit can be used in rapid screening of cynuthrin residue in Chinese cabbage.

Key words: Chinese cabbage; cynuthrin residue; rapid kit; evaluation

中图分类号:

S634.3

谭慧林, 金永生, 余琪, 牛贵洋, 包东东, 陈海元, 张志东. 大白菜中氟氯氰菊酯残留的快速测定及方法评估[J]. 新疆农业科学, 2021, 58(1): 168-175.

TAN Huilin, JIN Yongsheng, YU Qi, NIU Guiyang, BAO Dongdong, CHEN Haiyuan, ZHANG Zhidong. Determination of Cynuthrin Residues in Chinese Cabbages and Evaluation of the Rapid Detection Method[J]. Xinjiang Agricultural Sciences, 2021, 58(1): 168-175.

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大白菜中氟氯氰菊酯残留的快速测定及方法评估

Determination of Cynuthrin Residues in Chinese Cabbages and Evaluation of the Rapid Detection Method

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